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重氮化过程的危险性分析 | 2010-12-15 8:26:00
重氮化是使芳伯胺变为重氮盐的反应。通常是把含芳胺的有机化合物在酸性介质中与亚硝酸钠作用,使其中的胺基(-NH2)转变为重氮基(-N=N-)的化学反应。如二硝基重氮酚的制取等。 ^e\$\?I
重氮化的火灾危险性分析: s $T/d2xC
(1)重氮化反应的主要火灾危险性在于所产生的重氮盐,如重氮盐酸盐(C6H5N2Cl)、重氮硫酸盐(C6H5N2H504),特别是含有硝基的重氮盐,如重氮二硝基苯酚[(NO2)2N2C 6H2OH]等,它们在温度稍高或光的作用下,即易分解,有的甚至在室温时亦能分解。一般每升高 10℃ ,分解速度加快两倍。在干燥状态下,有些重氮盐不稳定,活力大,受热或摩擦、撞击能分解爆炸。含重氮盐的溶液若洒落在地上、蒸汽管道上,干燥后亦能引起着火或爆炸。在酸性介质中,有些金属如铁、铜、锌等能促使重氮化合物激烈地分解,甚至引起爆炸。 ;V]'#cA<
(2)作为重氮剂的芳胺化合物都是可燃有机物质,在一定条件下也有着火和爆炸的危险。 t\?azvj
(3)重氮化生产过程所使用的亚硝酸钠是无机氧化剂,于175℃ 时分解能与有机物反应发生着火或爆炸。亚硝酸钠并非氧化剂,所以当遇到比其氧化性强的氧化剂时,又具有还原性,故遇到氯酸钾、高锰酸钾、硝酸铵等强氧化剂时,有发生着火或爆炸的可能。 ckU=so
(4)在重氮化的生产过程中,若反应温度过高、亚硝酸钠的投料过快或过量,均会增加亚硝酸的浓度,加速物料的分解,产生大量的氧化氮气体,有引起着火爆炸的危险。 h V:3RPkU
wr>| 6NoC
重氮化的火灾危险性分析: s $T/d2xC
(1)重氮化反应的主要火灾危险性在于所产生的重氮盐,如重氮盐酸盐(C6H5N2Cl)、重氮硫酸盐(C6H5N2H504),特别是含有硝基的重氮盐,如重氮二硝基苯酚[(NO2)2N
(2)作为重氮剂的芳胺化合物都是可燃有机物质,在一定条件下也有着火和爆炸的危险。 t\?azvj
(3)重氮化生产过程所使用的亚硝酸钠是无机氧化剂,于
(4)在重氮化的生产过程中,若反应温度过高、亚硝酸钠的投料过快或过量,均会增加亚硝酸的浓度,加速物料的分解,产生大量的氧化氮气体,有引起着火爆炸的危险。 h V:3RPkU
wr>| 6NoC
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